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J Am Chem Soc 2010;132:8697–8703. [63] (a) Ruban AV, Skriver HL, Norskov JK. Phys Rev B 1999;59:15990–16000. (b) Maillet T, Barbier J, Gelin P, Praliaud H, Duprez D. J Catal 2001;202:367–378. (c) Skriver HL, Rosengaard NM. Phys Rev B 1992;46:7157–7168. [64] Salmeron M, Brewer L, Somorjai GA. Surf Sci 1981;112:207–228. [65] Andersson KJ, Calle-Vallejo F, Rossmeisl J, Chorkendorff L. J Am Chem Soc 2009;131:2404–2407. [66] Knudsen J, Nilekar AU, Vang RT, Schnadt J, Kunkes EL, Dumesic JA, Mavrikakis M, Besenbacher F.

The following section will survey the various cluster sources utilized in the field of cluster beam techniques. Methods 34 Physical Fabrication of Nanostructured Heterogeneous Catalysts of mass analysis and size selection will also be detailed. To conclude, selected ­experimental apparatus will be described to provide a full understanding of the complexities and capabilities of such instruments. 2 Cluster Sources Formation of metal clusters can be traced as far back as ancient Egypt and Rome where gold clusters were created during the long annealing of gold-doped glass to produce a ruby color.

This strategy is usually used for reaction ­mixtures with mild reducing agents, as the sequential reduction of two metal ­precursors depends on the difference in reduction potentials of the metal ions. For example, ­coreduction of Pt and Ru ions leads to the formation of Pt@Ru core–shell ­nanoparticles due to the high reduction potential of Pt ions [52a]. 2 Electrochemical Methods to Core–Shell Nanostructures Underpotential deposition (UPD) is one useful way to the fabrication of metal monolayer on metal nanoparticles [57].

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